节点文献
2,4—二硝基氟苯液相选择性催化氢化的研究
Reasearch an Selectire Catalgtic Hydrogenation of2,4-Dinitrofluorobensene in Liquid Phase
【摘要】 研究以 Pd Cl2/ C+ Fe( O Ac)2 为催化剂,乙酸和乙醇为溶剂,在室温和低压下用氢气选择性还原2 ,4 - 二硝基氟苯为2 - 氟- 5 - 硝基苯胺,选择性还原收率为76 .1 % ,产品纯度为99 .0 % 。
【Abstract】 The method for the catalytic selective reduction of 2,4-dinitrofluorobenzene in the presence of pdcl 2/c+Fe(oAc) 2 and hydrogen is studied.The reduction reaction is carried out in an acidic medium at room tempreature and low pressure.The yield of 2-fluoro-5-nitro-aniline is 76.1% and the parity is 99.0%.
- 【文献出处】 安徽大学学报(自然科学版) ,JOURNAL OF ANHUI UNIVERSITY(NATURAL SCIENCES) , 编辑部邮箱 ,1999年03期
- 【被引频次】6
- 【下载频次】89