节点文献
三氨基三硝基苯甲苯母液成分的气相色谱-质谱分析
Analysis of the Component of Toluene Solution of Triaminotrinitrobenzene by Gas Chromatography-Mass Spectrometry
【Author】 XU Rui-juan, JIANG Yan, QIN Jun-yong (Institute of Chemical Materials, China Academy of Engineering Physics, Mianyang 621900, China)
【机构】 中国工程物理研究院化工材料研究所;
【摘要】 <正> 1,3,5-三氨基-2,4,6-三硝基苯(TATB)是一种钝感高能炸药,其合成过程通常是采用硝酸和发烟硫酸硝化1,3,5-三氯苯(TCB)得到1,3,5-三氯-2,4,6-三硝基苯(TCTNB),然后将TCTNB的甲苯溶液进行胺化反应得到终产物TATB。
【Abstract】 In order to know some organic byproducts formed during composing 1,3,5-triamion-2,4, 6-trinitrobenzene (TATB), the components in toluene mother solution of TATB were separated and identified by gas chromatography—mass spectrometry (GC/MS). The results showed that the impurities of trichlorodinitrobenzene, trichlorotrinitrobenzene, tetrachlorodinitrobenzene, dinichlorotrinitroaniline and trichlorodinitroaniline presented in toluene solution of TATB.
- 【会议录名称】 中国质谱学会第七届会员代表大会暨学术报告会论文集
- 【会议名称】中国质谱学会第七届会员代表大会暨学术报告会
- 【会议时间】2004-10
- 【会议地点】中国广西北海
- 【分类号】O657.63
- 【主办单位】中国质谱学会