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GC/MS法检测苯系物

Detection of Aromatic Hydrocarbon Compounds in Water by GC/MS

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【作者】 宋鸣王成明

【Author】 SONG Ming~1 WANG Cheng-ming~2 (1.Liaoning Criminal Science and Technology Research Institute,Shenyang 110032,China;2.Fuxin Municipal Public Security Bureau,Fuxin 123000,China)

【机构】 辽宁省刑事科学技术研究所阜新市公安局刑侦支队

【摘要】 <正>从水中提取有机物的常用方法为有机溶剂液-液提取法,此法操作繁琐,且由于苯系物具较大的挥发性,在挥散溶剂时易造成被测组分损失。固相萃取法在柱上净化富集样品,具有提取效率高、基质干扰小等特点,适用于水中苯系物的提取,是近年来应用广泛的样品提取技术。气相色谱-质

【Abstract】 A method was developed for determing aromatic hydrocarbon compounds in polluted water.The aromatic hydrocarbon compounds were isolated and enriched from water samples by solid-phase extraction with C18 carridge and detected by gas chromatography-mass spectrometry.Several aromatic hydrocarbon compounds including trimethyibenzene,tetramethyibenzens and diethylbenzene in polluted water samples could be detected simultaneously.The detection limit for toluene,trimethylbenzene and tetramethylbenzene were 10 μg·L-1. Detected by this method,several aromatic hydrocarbon compounds were detected in a polluted water sample.

  • 【会议录名称】 中国有机质谱学第十四届全国学术大会会议论文集
  • 【会议名称】中国有机质谱学第十四届全国学术大会
  • 【会议时间】2007-11
  • 【会议地点】中国上海
  • 【分类号】X132
  • 【主办单位】中国质谱学会有机质谱专业委员会
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