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CdS光催化剂的水热两步制备及其产氢活性研究

Preparation of CdS Photocatalyst and Its Performance of Hydrogen Production

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【作者】 张相辉敬登伟邢婵娟郭烈锦

【Author】 ZHANG Xiang-hui,JING Deng-wei, XING Chan-Juan , GUO Lie-Jin (State Key Laboratory of Multiphase Flow in Power Engineering,Xi’an Jiaotong University,Xi’an 710049, China)

【机构】 西安交通大学动力工程多相流国家重点实验室

【摘要】 用水热法分一步和两步分别制备了CdS光催化剂。对所制备的光催化剂进行载Pt实验,得到了其最佳载Pt量。用XRD、UV-Vis、XRF、SEM和TEM对光催化剂结构进行表征分析,并测试了其在可见光下的产氢量, 发现两步法制备的光催化剂产氢活性有明显提高。

【Abstract】 Cadmium sulfide photocatalyst was prepared by hydrothermal methods with one-step and two-step methods, respectively. Platinum was loaded on the surface of prepared photocatalysts and its optimal loading amount was examined. All the prepared photocatalysts were characterized by XRD,UV-Vis, XRF, SEM and TEM and their pohtocatalytic activity was evaluated by H2 evolution from water under visible light. It was found that the photocatalyst prepared by two-step showed markedly improved hydrogen production activity.

【关键词】 CdS光催化剂产氢
【Key words】 CdSphotocatalysthydrogen production
【基金】 973计划(2003CB21450);国家自然科学基金(50521604).
  • 【会议录名称】 第七届全国氢能学术会议论文集
  • 【会议名称】第七届全国氢能学术会议
  • 【会议时间】2006-11
  • 【会议地点】中国湖北武汉
  • 【分类号】TQ116.2
  • 【主办单位】中国可再生能源学会氢能专业委员会
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