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毛细管电泳非接触电导分离检测金属氧化物纳米粒子
Separation of nanoparticles of metal oxides by capillary electrophoresis with contactless conductivity detection
【Author】 Guan Liao1, WANG Li-xin2, FU Chong-gang*1 1School of chemistry and chemical engineering, Liaocheng University;2School of Media and communications Technology, Liaocheng University, Liaocheng 252059
【机构】 聊城大学化学化工学院; 聊城大学传媒技术学院;
【摘要】 <正>采用毛细管电泳非接触电导检测技术,以碳酸钠-碳酸氢钠为缓冲体系,同时分离测定了纳米TiO2和Al2O3两种金属氧化物的悬浮粒子。考察了缓冲溶液种类、浓度及pH对分离效果的影响,
【Abstract】 The separation of two-component mixture composed of TiO2 and Al2O3 nanoparticles suspended in carbonate buffer solution was achieved by capillary electrophoresis with contactless conductivity detection. The effects of variety, concentration and pH of running buffer solutions on separation were investigated. The effects of amptitude and frequency of exitation signal on signal-to-noise ratio were also studied. Under optimized conditions, the complete separation of nanoparticles of TiO2 and Al2O3 were accomplished within 8 min.
【Key words】 Capillary electrophoresis; Contactless conductivity detection; Metal oxides; Nanoparticle;
- 【会议录名称】 中国化学会第26届学术年会分析化学分会场论文集
- 【会议名称】中国化学会第26届学术年会分析化学分会场
- 【会议时间】2008-07
- 【会议地点】中国天津
- 【分类号】O658.9
- 【主办单位】中国化学会