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氰乙酸甲酯化工艺条件的研究

Studies 0n Esterification of Methyl cyanoacetate

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【作者】 盖丽芳尚会建彭丽敏郑学明

【Author】 Li-Fang Ge,Hui-Jian Shang,Li-Min Peng,Xue-Ming Zheng* HeBei University of Science and Technology,050018,Shijiazhuang

【机构】 河北科技大学

【Abstract】 Esterification of methyl cyanoacetate was a complicated reaction network.It included the reversible-consecutive-parallel reaction. The reaction rule for methyl cyanoacetate has been less reported. Esterification process of methyl cyanoacetate was studied in this paper. The effects of resction temperature, the amount of the catalyst and the ratio of methyl alcohol to cyanoacetic acid were investigated. Results suggest that the optimum esterification conditions are as foIlows: resction temperature :70℃. the amount of the catalyst : 7%. the ratio of methyl alcohol to cyanoacetic acid: 4:1.

【关键词】 氰乙酸氰乙酸甲酯反应规律
  • 【会议录名称】 中国化学会第二十五届学术年会论文摘要集(上册)
  • 【会议名称】中国化学会第二十五届学术年会
  • 【会议时间】2006-07
  • 【会议地点】中国吉林长春
  • 【分类号】TQ225.24
  • 【主办单位】中国化学会
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