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氯化锌催化下C60与枞酸的反应及产物结构研究
Studies on Reaction and Product Structure of C60 with Abietic Acid in Presence of ZnCl2
【Author】 Zhong-Xiang Lin*, Xia Ding,Hui-Ming Deng College of Chemical Engineering ,Nanjing Forestry University,210037,Nanjing
【机构】 南京林业大学化工学院；
【Abstract】 The reaction of C60 with abietic acid in the presence of ZnCl2 in o-dichlorobenzene at 175～180℃ for 8 h afforded C60 adducts that was expected to be Diels-Alder adducts of C60 with pimaric acid. The C60 adducts were isolated by silica column chromatography and characterized by FT-IR、13C NMR、1H NMR、MALDI-TOF-MS. The results showed that dehydrogenation and decarboxylation take placed and afford C60 adducts with aromatic group in this reaction.
- 【会议录名称】 中国化学会第二十五届学术年会论文摘要集（上册）
- 【会议名称】中国化学会第二十五届学术年会
- 【会议时间】2006-07
- 【会议地点】中国吉林长春
- 【分类号】O643.32
- 【主办单位】中国化学会