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微波辐射无溶剂快速合成2-羟基苯并咪唑

Synthesis of 2-Hydroxy benzimidazole in Solventless System Under Microwave Irradiation

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【作者】 常慧宁满侠

【Author】 Hui Chang *, Man-Xia Ning Department of Chemistry and Biology Engineering Dong Guan University of technology , 523106 Dong Guan

【机构】 东莞理工学院化学生物工程系

【Abstract】 2-hydrxybenzimidazole were synthesized by the condensation reaction of urea and o-phenylenediamine under microwave irradiation solventless condition . The reaction was fast , Operation was simple.,The optimum conditions were microwave power 638W , microwave irradiation time 9min , the mol ratio of o-phenylendiamin and urea 1︰1.1 , The yield was 88.5% .Their formular and struactiure were identification by IR Spectroscopy analysis .

  • 【会议录名称】 中国化学会第二十五届学术年会论文摘要集(上册)
  • 【会议名称】中国化学会第二十五届学术年会
  • 【会议时间】2006-07
  • 【会议地点】中国吉林长春
  • 【分类号】O626.23
  • 【主办单位】中国化学会
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