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高锰TWIP钢退火过程组织演变机理及力学性能

Microstructural evolution mechanisms and mechanical properties of high-manganese TWIP steel during annealing

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【作者】 杨璐张韵沈晓辉刘伟明魏海莲潘红波

【Author】 YANG Lu;ZHANG Yun;SHEN Xiao-hui;LIU Wei-ming;WEI Hai-lian;PAN Hong-bo;Anhui Key Laboratory of Low Carbon Metallurgy and Solid Waste Resources Utilization, Anhui University of Technology;School of Metallurgical Engineering, Anhui University of Technology;School of Materials Science and Engineering,Anhui University of Technology;

【通讯作者】 潘红波;

【机构】 安徽工业大学安徽省低碳冶金与固废资源化利用重点实验室安徽工业大学冶金工程学院安徽工业大学材料科学与工程学院

【摘要】 针对高锰钢高加工硬化特性导致工业大压下率冷轧难以进行的现状,基于工业可行冷轧压下率(30%)对高锰TWIP钢进行冷轧,随后对其进行750和900℃退火保温不同时间的处理,获得不同比例(0%~100%)细晶镶嵌于粗晶基体中的单相奥氏体异质结构,分析了不同退火工艺下试验钢的再结晶形核机制。结果表明:在750℃退火保温300 s后,试验钢的组织主要由变形奥氏体和粗晶奥氏体构成,随着保温时间延长到1800 s,变形奥氏体逐渐通过亚晶合并形核的方式发生再结晶;在900℃退火保温300 s时,晶界形核占据主导地位,而保温时间延长到1800 s后,组织逐渐转变为等轴晶粒;其中,在900℃退火保温300 s后,试验钢得到了再结晶体积分数为30%的异质结构组织,在形变过程中通过位错塞积与孪晶诱导塑性(TWIP)效应协同作用,实现高强度与高塑性的优异匹配,其屈服强度与抗拉强度分别为611.1和915.6 MPa,同时保持52.5%的伸长率,强塑积达到48 GPa·%。

【Abstract】 In response to the difficulty of industrial cold rolling with high reduction rates caused by the high work hardening characteristics of high-manganese steel, cold rolling treatment with a feasible industrial cold rolling reduction rate(30%) was carried out on high-manganese TWIP steel. Subsequently, it was annealed at 750 ℃ and 900 ℃ for different time to obtain a single-phase austenite heterogeneous structure where different proportions(0%-100%) of fine grains were embedded in a coarse grain matrix. The recrystallization nucleation mechanism of the experimental steel under different annealing processes was analyzed. The results show that after annealing at 750 ℃ for 300 s, the microstructure of the experimental steel is mainly composed of deformed austenite and coarse-grained austenite. As the holding time increases to 1800 s, the deformed austenite gradually undergoes recrystallization through subgrain coalescence and nucleation. When annealed at 900 ℃ for 300 s, grain boundary nucleation dominates, while after the holding time increases to 1800 s, the microstructure gradually transforms into equiaxed grains. Among them, after annealing at 900 ℃ for 300 s, the experimental steel obtains a heterogeneous structure with a recrystallization volume fraction of 30%. During the deformation, the synergistic effect of dislocation pile-up and twin-induced plasticity(TWIP) is achieved, enabling an excellent match between high strength and high plasticity: the yield strength and tensile strength are 611.1 and 915.6 MPa, respectively, while maintaining an elongation of 52.5%, and the product of strength and elongation reaches 48 GPa·%.

【基金】 国家自然科学基金(U1860105,52404334);安徽省高校自科重大项目(2024AH040025);安徽省重点研发计划项目(202304a05020026)
  • 【文献出处】 材料热处理学报 ,Transactions of Materials and Heat Treatment , 编辑部邮箱 ,2026年02期
  • 【分类号】TG142.1
  • 【下载频次】33
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