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氦同位素4 K低温吸附分离特性研究
Research on cryogenic adsorptive separation characteristics of helium isotopes at 4 K
【摘要】 为发展自主可控的3He/4He分离技术,研制了一套以GM制冷机为冷源的氦同位素低温吸附分离实验平台,主要部件包括低温控制单元、气体控制单元以及吸附柱单元。选用椰壳活性炭作为吸附剂,通过动态吸附-解吸循环实验探究其对3He/4He混合气体的分离特性。实验结果表明:在4.2 K的吸附温度下,3He在椰壳活性炭上的动态吸附性能显著优于4He;经过3次连续的吸附-解吸循环后,所得解吸气体中3He的丰度由初始值提升至99.93%。
【Abstract】 To advance the development of autonomous and controllable 3He /4He separation technology, an experimental cryogenic adsorption separation platform for helium isotopes was established, utilizing a GM cryocooler as the cold source. The primary components of the system include a cryogenic control unit, a gas control unit, and an adsorption column unit. Coconut shell activated carbon was selected as the adsorbent, and its separation characteristics for 3He /4He gas mixtures were investigated through dynamic adsorption-desorption cycle experiments. The experimental results indicate that at an adsorption temperature of 4. 2 K, the dynamic adsorption performance of 3He on coconut shell activated carbon is significantly superior to that of 4He. After three consecutive adsorption-desorption cycles, the 3He abundance in the desorbed gas increased from the initial value to 99. 93%.
【Key words】 cryogenic separation of helium isotopes; 4 K adsorption; ultra-high-purity helium-3 extraction;
- 【文献出处】 低温工程 ,Cryogenics , 编辑部邮箱 ,2026年01期
- 【分类号】TL921;O647.3;TB651
- 【下载频次】17