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某石墨矿综合回收石墨及伴生钒矿试验研究

Experimental study on comprehensive recovery of graphite and associated vanadium ore from a graphite mine

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【作者】 刘建国戴惠新于丽丽冯嘉颖王在华

【Author】 LIU Jianguo;DAI Huixin;YU Lili;FENG Jiaying;WANG Zaihua;Faculty of Land Resources Engineering,Kunming University of Science and Technology;Institute of Resources Utilization and Rare Earth Development,Guangdong Academy of Sciences;State Key Laboratory of Separation and Comprehensive Utilization of Rare Metals;Guangdong Key Laboratory of Mineral Resources Development and Comprehensive Utilization;

【通讯作者】 戴惠新;

【机构】 昆明理工大学国土资源工程学院广东省科学院资源利用与稀土开发研究所稀有金属分离与综合利用国家重点实验室广东省矿产资源开发与综合利用重点实验室

【摘要】 国外某石墨钒矿,原矿固定碳含量15.30%、V2O5含量0.51%,以石墨矿回收为主,伴生回收主要含钒矿物钒云母,石墨矿嵌布粒度粗,钒云母嵌布粒度细。对该石墨钒矿进行了石墨浮选-钒云母浮选选矿试验研究,得到适宜的石墨粗选及粗精矿磨矿细度条件:粗选磨矿细度-0.074 mm占52.66%,捕收剂为煤油与石蜡油1∶1的混合油,用量为70 g/t,水玻璃用量1 500 g/t,粗精矿再磨细度-0.074 mm占60.04%;适宜的钒云母粗选及粗精矿磨矿细度条件:粗选捕收剂为P8X,用量为200 g/t,粗精矿磨矿细度-0.074 mm占74.35%,矿样采用一粗三扫四精石墨浮选-一粗二扫二精钒云母浮选流程进行闭路试验,最终获得石墨精矿固定碳含量96.63%、回收率96.28%,以及钒云母精矿V2O5含量1.86%、回收率83.41%的选别指标,为该类矿石综合回收石墨、钒矿提供了技术参考。

【Abstract】 A graphite-vanadium ore is from a foreign country,the fixed carbon content of the raw ore is 15.30%,with the V2O5 content of 0.51%,the graphite ore is mainly recovered ore,and accompanying the recovery of vanadium-containing mineral,which is roscoelite,the dissemination of graphite is coarse,and the dissemination of roscoelite is fine.The separation tests are carried out about graphite flotation-roscoelite flotation for the raw ore,the suitable separation parameters of graphite separation are obtained:the grinding fineness of rougher is -0.074 mm 52.66%,the collector of graphite is the mixture oil of kerosene∶paraffin oil=1∶1,and the dosage is 70 g/t for rougher with the water glass of 1 500 g/t,the regrinding fineness of rougher concentrate is-0.074 mm 60.04%.And the suitable separation parameters of roscoelite separation are obtained too.The collector of roscoelite is P8X with the dosage of 200 g/t,the grinding fineness of rougher concentrate is -0.074 mm 74.35%.The closedcircuit test is carried out with the testing procedures of one roughing,three scavenging and four cleaning graphite flotation-one roughing,two scavenging and two cleaning roscoelite flotation,and the separation indexes can be obtained,the fixed carbon content of graphite concentrate is 96.63%with the recovery rate of 96.28%,and the V2O5 content of roscoelite concentrate is 1.86% with the recovery rate of 83.41%,the research results provide a technical reference for the comprehensive recovery of this type of graphite-vanadium ore.

【基金】 广东省基础与应用基础研究基金项目资助(编号:2022A1515012165);广东省重点领域研发计划项目资助(编号:2022B0303030002)
  • 【文献出处】 中国矿业 ,China Mining Magazine , 编辑部邮箱 ,2025年01期
  • 【分类号】TD97;TD923
  • 【下载频次】36
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