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Preparation and Properties of Ti3SiC2-modified High Silica/Phenolic Aerogel Composite

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【作者】 曹文静LIU YimingZHAO DongmeiWAN XiaoboLIU YangHUANG Kun石敏先

【Author】 CAO Wenjing;LIU Yiming;ZHAO Dongmei;WAN Xiaobo;LIU Yang;HUANG Kun;SHI Minxian;School of Materials Science and Engineering, Wuhan University of Technology;Wuhan Haiwei Ship and Ocean Engineering Technology Co., Ltd.;

【通讯作者】 石敏先;

【机构】 School of Materials Science and Engineering, Wuhan University of TechnologyWuhan Haiwei Ship and Ocean Engineering Technology Co., Ltd.

【摘要】 A Ti3SiC2-modified high-silica oxygen/phenolic aerogel composite with excellent oxidation resistance and high-temperature performance was prepared.The experimental results show that the obtained composite has significantly improved oxidation resistance.When the addition amount of Ti3SiC2 is 75%,the carbonization volume shrinkage rate of the composite after aerobic static combustion is only 5.95%.At the same time,the LAR and MAR after 30 seconds of oxyacetylene ablation under a heat flux density of 1.5 MW/m2 are 0.0307 mm/s and 0.0149 g/s,respectively.The compressive strength after aerobic static combustion at 1 000 ℃ is up to 20.43% of that before aerobic static combustion,which is 1.99 times that of the unfilled material,significantly improving the high-temperature mechanical properties of the composite.

【Abstract】 A Ti3SiC2-modified high-silica oxygen/phenolic aerogel composite with excellent oxidation resistance and high-temperature performance was prepared.The experimental results show that the obtained composite has significantly improved oxidation resistance.When the addition amount of Ti3SiC2 is 75%,the carbonization volume shrinkage rate of the composite after aerobic static combustion is only 5.95%.At the same time,the LAR and MAR after 30 seconds of oxyacetylene ablation under a heat flux density of 1.5 MW/m2 are 0.0307 mm/s and 0.0149 g/s,respectively.The compressive strength after aerobic static combustion at 1 000 ℃ is up to 20.43% of that before aerobic static combustion,which is 1.99 times that of the unfilled material,significantly improving the high-temperature mechanical properties of the composite.

【基金】 Funded by by the Wuhan Science and Technology Project (No.2024010702030141)
  • 【文献出处】 Journal of Wuhan University of Technology(Materials Science) ,武汉理工大学学报(材料科学版)(英文版) , 编辑部邮箱 ,2025年06期
  • 【分类号】TB332
  • 【下载频次】6
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