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光固化Si3N4陶瓷料浆的流变性能研究

Study on the rheological properties of photocurable Si3N4 ceramic slurries

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【作者】 韩卓群周庆旋李佳齐张霞毕鲁南王浩李伶

【Author】 HAN Zhuoqun;ZHOU Qingxuan;LI Jiaqi;ZHANG Xia;BI Lunan;WANG Hao;LI Ling;Shandong Industrial Ceramics Research & Design Institute Co., Ltd.;

【机构】 山东工业陶瓷研究设计院有限公司

【摘要】 围绕Si3N4陶瓷粉体在光敏树脂中的分散与固化行为,系统研究了树脂配方、分散剂种类及掺加量等因素对陶瓷浆料流变性能和光固化性能的影响。结果显示,合适的不同官能度树脂配比可有效提升浆料的流变性能和固化性能;选用适宜的分散剂种类并控制其掺加量,有助于改善Si3N4陶瓷粉体在树脂中的分散稳定性,从而降低浆料黏度,为高固化厚度、高固含量Si3N4陶瓷浆料的光固化增材制造提供了理论支撑与工艺指导。

【Abstract】 This study systematically investigates the dispersion and curing behavior of Si3N4 ceramic powders in a photocurable resin system, focusing on the effects of resin formulation, dispersant type, and dosage on the rheological and photocuring properties of ceramic slurries. The results show that a rational combination of resins with different functionalities can significantly enhance both slurry flowability and curing depth. Moreover, selecting appropriate dispersants and optimizing their addition effectively improves the dispersion stability of Si3N4 powders in the resin matrix, thereby reducing slurry viscosity. This work provides theoretical support and process guidance for the development of high-solid-loading, high-curing-depth Si3N4 ceramic slurries for photocuring-based additive manufacturing.

【基金】 国家重点研发计划项目(编号:2022YFB3706300);山东省重点研发计划项目(编号:2024CXPT018)
  • 【文献出处】 中国建材科技 ,China Building Materials Science & Technology , 编辑部邮箱 ,2025年S1期
  • 【分类号】TQ174.1
  • 【下载频次】24
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