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冷轧、退火和时效对Fe50Ni25Cr15Al10高熵合金组织和性能的影响

Effect of cold rolling, annealing and aging on microstructure and properties of Fe50Ni25Cr15Al10 high entropy alloy

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【作者】 邢振强庞景宇张宏伟纪宇朱正旺张龙王爱民张海峰

【Author】 Xing Zhenqiang;Pang Jingyu;Zhang Hongwei;Ji Yu;Zhu Zhengwang;Zhang Long;Wang Aimin;Zhang Haifeng;School of Materials Science and Engineering, Dalian Jiaotong University;Shi-changxu Innovation Center for Advanced Materials, Institute of Metal Research,Chinese Academy of Sciences;School of Metallurgy, Northeastern University;

【通讯作者】 庞景宇;

【机构】 大连交通大学材料与工程学院中国科学院金属研究所师昌绪先进材料创新中心东北大学冶金学院

【摘要】 研究了冷轧、退火和时效对Fe50Ni25Cr15Al10高熵合金组织和力学性能的影响。结果表明,铸态Fe50Ni25Cr15Al10高熵合金为FCC+B2双相结构。冷轧、退火和时效后,FCC相由树枝晶转变为等轴晶,并产生占比约为43.7%的退火孪晶,平均晶粒尺寸从228.84μm细化到4.51μm。B2相呈现出两种析出方式,分别是沿晶析出的链状大尺寸相和晶内弥散分布的小尺寸椭球形相,并且B2相占比从0.9%提升至13.3%。结构的调控使合金的屈服强度和抗拉强度分别由铸态的254 MPa和528 MPa提高到466 MPa和760 MPa,断裂总延伸率为31.5%,具有良好的强塑性匹配。

【Abstract】 Effects of cold rolling, annealing and aging on the microstructure and mechanical properties of the Fe50Ni25Cr15Al10 high entropy alloy were investigated. The results show that the as-cast Fe50Ni25Cr15Al10 high entropy alloy has FCC+B2 bi-phase structure. After cold rolling, annealing and aging, the FCC phase is transformed from dendrite to equiaxial grains, the annealing twins accounting for 43.7% are produced, and the average grain size is refined from 228.84 μm to 4.51 μm. The B2 phase exhibits two precipitation modes, namely chain like large-sized intergranular precipitated phase and small-sized ellipsoidal phase dispersing inside the grains, and the proportion of B2 phase increases from 0.9% to 13.3%. The yield strength and tensile strength of the high entropy alloy are increased from 254 MPa and 528 MPa to 466 MPa and 760 MPa, respectively, and the percentage total extension at fracture is 31.5%, showing good strength-plasticity matching.

【基金】 辽宁省应用基础研究计划(2022JH2/101300080);中国科学院项目(ZDBS-LY-JSC023);辽宁省自然科学基金(2023-BS-012);中国科学院金属研究所创新基金(2023-PY16)
  • 【文献出处】 金属热处理 ,Heat Treatment of Metals , 编辑部邮箱 ,2024年05期
  • 【分类号】TG139;TG156;TG335.12
  • 【下载频次】110
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