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振荡热压烧结ZrB2–SiC陶瓷的力学性能
Mechanical Properties of ZrB2–SiC Ceramics Sintered by Hot Oscillatory Pressing
【摘要】 采用振荡热压烧结(HOP)和热压烧结(HP)工艺制备了ZrB2–SiC陶瓷,研究了振荡压力对ZrB2–SiC陶瓷致密化及力学性能的影响。结果表明,与采用HP工艺制备ZrB2–SiC陶瓷相比,HOP工艺的致密化速率有显著提升;ZrB2与SiC两相界面结合良好;HOP工艺制备的ZS30样品的硬度和断裂韧性分别达到了21.1 GPa和7.3MPa·m1/2,较采用HP工艺在相同烧结参数下制备的试样有大幅提升。HOP在制备高性能ZrB2–SiC陶瓷方面展现出良好发展前景。
【Abstract】 ZrB2–SiC ceramics were prepared using hot oscillatory pressing(HOP) and hot pressing(HP processes, and the effect of oscillatory pressure on the densification and mechanical properties of ZrB2–SiC ceramics was investigated. The results have shown that compared to using the HP process to fabricate ZrB2–SiC ceramics, the densification rate of HOP process has been improved significantly, and the interface between ZrB2 and SiC is well bonded; The hardness and fracture toughness of the ZS30 sample prepared by the HOP process reached 21.1 GPa and 7.3 MPa·m1/2, respectively, which were significantly improved compared to the samples prepared by the HP process under the same sintering parameters. HOP has shown good development prospects in the preparation of high-performance ZrB2–SiC ceramics.
【Key words】 Ultra-high temperature ceramics(UHTCs); ZrB2; Sintering; Densification; Mechanical properties;
- 【文献出处】 航空制造技术 ,Aeronautical Manufacturing Technology , 编辑部邮箱 ,2024年13期
- 【分类号】TQ174.1
- 【下载频次】7