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电感耦合等离子体发射光谱法测定蒙脱石中钛含量

Determination of Titanium Content in Montmorillonite by Inductively Coupled Plasma Optical Emission Spectrometry

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【作者】 马继承马婧王爱霞

【Author】 Ma Jicheng;Ma Jing;Wang Aixia;Faculty of Chemistry, Northeast Normal University;Jilin Provincial Experimental School;

【通讯作者】 马继承;

【机构】 东北师范大学化学学院吉林省实验中学

【摘要】 本研究建立了电感耦合等离子体发射光谱法(ICP-OES)测定蒙脱石中钛(Ti)元素含量的检测方法。实验结果表明该方法线性关系良好,相关系数(r)大于0.999;钛元素的检出限和定量限分别为0.0965和0.318 mg·kg-1;精密度和重复性的相对标准偏差(RSD)分别为0.676%和2.29%,加标回收率为99.69%。以上结果说明该方法检出限低,精密度和准确度高,是检测蒙脱石以及类似矿物样品钛元素的理想分析方法。

【Abstract】 A detection method for determining titanium in montmorillonite by inductively coupled plasma optical emission spectroscopy(ICP-OES) has been established. The experimental results show that the method has a good linear relationship, and the correlation coefficient(r) is greater than 0.999; The detection limit and quantification limit of titanium element are 0.0965 and 0.318 mg·kg-1, respectively; The relative standard deviation(RSD) of precision and repeatability were0.676 % and 2.29 %, respectively, and the recovery rate of samples was 99.69 %. The above results indicate that this method has a low detection limit, high precision and accuracy, and is an ideal analytical method for detecting titanium elements in montmorillonite and similar mineral samples.

【基金】 吉林省教育厅科学技术研究项目(JJKH20231303KJ)
  • 【文献出处】 广东化工 ,Guangdong Chemical Industry , 编辑部邮箱 ,2024年18期
  • 【分类号】P575;O657.31
  • 【下载频次】48
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