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Fe3O4-Cell-PGMA-PEI的制备及其对水中Pb2+的吸附研究

Study on the Preparation of Fe3O4-Cell-PGMA-PEI and Its Adsorption of Pb(Ⅱ) in Water

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【作者】 王中华刘明源陈亚运刘智

【Author】 WANG Zhong-hua;LIU Ming-yuan;CHEN Ya-yun;LIU Zhi;Taizhou Polytechnical Institute;Taizhou Green Chemical Engineering Technology Center;

【机构】 泰州职业技术学院泰州市绿色化工工程技术中心

【摘要】 以纤维素为原料,采用共沉淀法将Fe3O4粒子负载于纤维素中,然后用甲基丙烯酸缩水甘油酯与磁性纤维素进行接枝共聚,再与聚乙烯亚胺进行胺化反应,制得Fe3O4-Cell-PGMA-PEI,采用FT-IR、EA、XPS、TGA等方法对磁性吸附剂进行结构表征。在静态条件下,研究吸附剂用量、吸附时间、溶液初始p H、温度等因素对Fe3O4-Cell-PGMA-PEI吸附Pb2+效果的影响,确定吸附的最佳条件。

【Abstract】 Using cellulose as raw material,Fe3O4 particles were loaded into cellulose by coprecipitation method,then the magnetic cellulose was grafted with glycidyl methacrylate (GMA),and aminated with polyethylene imine (PEI) to prepare Fe3O4-Cell PGMA-PEI,its structure was characterized by FT-IR,FT-IR,EA,XPS,TG/DTG.Under static condition,the effects of the dosage of adsorbent,adsorption time,initial p H and temperature on the adsorption of Pb2+by Fe3O4-Cell-PGMA-PEI were studied,and the best adsorption conditions were determined.

【基金】 2021年度泰州市科技支撑计划(社会发展)项目,纤维素基多胺型螯合吸附剂对重金属Pb(II)的吸附研究(项目编号:202103)
  • 【文献出处】 当代化工 ,Contemporary Chemical Industry , 编辑部邮箱 ,2023年12期
  • 【分类号】TQ424;X703
  • 【下载频次】32
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