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黄姜花中二芳基庚烷的分离鉴定

Isolation and Identification of Diarylheptanes from Hedychium flavum

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【作者】 李敏余丽梅程浩李显莹刘波彭伟陈业高

【Author】 LI Min;YU Limei;CHENG Hao;LI Xianying;LIU Bo;PENG Wei;CHEN Yegao;School of Chemistry and Chemical Engineering, Yunnan Normal University;

【通讯作者】 陈业高;

【机构】 云南师范大学化学化工学院

【摘要】 风干的黄姜花(Hedychium flavum)根茎粉碎后,用工业甲醇浸泡提取。提取物水溶后用乙酸乙酯萃取,乙酸乙酯萃取部分利用柱层析和HPLC等方法进行分离,经NMR等方法鉴定后,得到4个二芳基庚烷类化合物,化合物分别为:1,7-bis(4-hydroxy-3-methoxyphenyl)heptane-3,5-diol (1)、5-hydroxy-1-(4’-hydroxyphenyl)-7-(4’’-hydroxy-3’’-methoxyphenyl)-3-heptanone (2)、gingerenone A (3)和coriandralpinin C (4),均为首次从黄姜花中分离得到。

【Abstract】 The rhizomes of dried Hedychium flavum were crushed, extracted with industrial methanol. The extract was dissolved with water and then extracted with ethyl acetate. The ethyl acetate part was separated by gel column chromatography and HPLC. Four diarylheptanes were obtained and identified by NMR, and the compounds were identified as 1,7-bis(4-hydroxy-3-methoxyphenyl)heptane-3,5-diol(1), 5-hydroxy-1-(4’-hydroxyphenyl)-7-(4’’-hydroxy-3’’-methoxyphenyl)-3-heptanone(2), gingerenone A(3) and coriandralpinin C(4). All the compounds were isolated for the first time from Hedychium flavum.

  • 【文献出处】 海南师范大学学报(自然科学版) ,Journal of Hainan Normal University(Natural Science) , 编辑部邮箱 ,2023年02期
  • 【分类号】R284.1
  • 【下载频次】9
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