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FSP制备TiO2铝基复合材料的组织与性能研究

Study on the microstructure and properties of TiO2/Al composites prepared by FSP

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【作者】 张亮王天顺徐鑫月王会霞崔伟

【Author】 ZHANG Liang;WANG Tianshun;XU Xinyue;WANG Huixia;CUI Wei;School of Materials Science and Engineering, Hebei University of Science and Technology;Hebei Key Laboratory of Materials Nearnet Forming Technology;Wangdu Hebei Technology Service Company Limited;

【机构】 河北科技大学材料科学与工程学院河北省材料近净成形技术重点实验室网都河北科技服务有限公司

【摘要】 为了解决铝基复合材料强韧性的问题,采用搅拌摩擦加工(friction stir processing, FSP)的方法制备TiO2铝基复合材料。分别采用显微组织观察试验、拉伸试验和显微硬度试验等方法,对复合材料的强化机理、显微组织以及力学性能进行表征与分析。结果表明,TiO2的加入对复合材料具有细化晶粒作用,FSP改变了铝合金的结晶形式,由无形核的连续性动态再结晶转变为颗粒刺激形核机制;FSP制备TiO2铝基复合材料的抗拉强度及显微硬度均得到了提高,当添加量达到4.8%(质量分数)时,复合材料的抗拉强度达到456 MPa,硬度值达到130 HV,与未添加颗粒相比较,分别提高了17%和16%,而延伸率仅下降了4%。FSP制备TiO2铝基复合材料不仅可以有效提高力学性能,可以改善强韧性不匹配的问题,研究结果可为新型复合材料的应用提供理论基础和技术参考。

【Abstract】 In order to solve the problem of strength and toughness of aluminum matrix composites, TiO2/Al matrix composites were prepared by friction stir processing(FSP). The experiments were carried out by microstructure observation test, tensile test and micro-hardness test to characterize and analyze the strengthening mechanism, microstructure and mechanical properties of composites. The results show that with the introduction of TiO2, the grain has been refined, and the crystalline form of Al is change from continuous dynamic recrystallization(CDRX) of invisible core to the particle-stimulated nucleation mechanism by FSP. The tensile strength and microhardness of the composite are improved. When the addition amount reaches 4.8%(mass fraction), the tensile strength is 456 MPa, and the hardness is 130 HV, which increases by 17% and 16%, respectively, compared with that of the unadded particles, and the elongation decreases only by 4%. TiO2 prepared by FSP can effectively improve the mechanical properties and improve the strength and toughness mismatch, which provides theoretical basis and technical reference for the application of new composite materials.

【基金】 河北省重点研发计划(19211016D);河北省重点研发计划项目(20351002D);国家自然科学基金(51775007);河北省高等学校科学技术研究项目(ZD2018060)
  • 【文献出处】 河北科技大学学报 ,Journal of Hebei University of Science and Technology , 编辑部邮箱 ,2023年04期
  • 【分类号】TB333
  • 【下载频次】3
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