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多不饱和脂肪酸油脂微胶囊的工艺优化

Process optimization of polyunsaturated fatty acid oil microcapsule

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【作者】 桂正杰熊友鹏黄启东周绪杨洁

【Author】 GUI Zheng-jie;XIONG You-peng;HUANG Qi-dong;ZHOU Xu;YANG Jie;College of Nursing and Health Management & College of Life Science and Chemistry,Wuhan Donghu University;Innovation Institute for Biomedical Materials,Wuhan Donghu University;College of Life Science and Technology,Huazhong University of Science and Technology;

【通讯作者】 杨洁;

【机构】 武汉东湖学院护理与健康管理学院(生命科学与化学学院)武汉东湖学院生物医用材料创新研究所华中科技大学生命科学与技术学院

【摘要】 目的:为顺应市场需求开发高浓度PUFA油脂微胶囊。方法:以β-环糊精/明胶为复合壁材,高含量多不饱和脂肪酸油脂葵花籽油为芯材,采用喷雾干燥法制备葵花籽油粉末微胶囊,并通过单因素试验和响应面试验优化油脂微胶囊制备工艺参数。结果:油脂微胶囊的最佳工艺条件为固形物含量25.2%、复合壁材配比(mβ-环糊精∶m明胶)6.7∶1、乳化剂用量1%、芯壁材配比(m葵花籽油∶m复合壁材)1∶2,在该工艺条件下得到的油脂微胶囊颗粒完整,粒径大小均匀,包埋率达94.33%,其中多不饱和脂肪酸含量达21.73%。结论:该制备方法可行,能够实现高浓度多不饱和脂肪酸油脂微胶囊的制备。

【Abstract】 Objective: To meet the market demand, high concentration PUFA oil microcapsules were developed. Methods: The microencapsulated oil was prepared by spray drying method with β-cyclodextrin/gelatin as a composite wall material and high content polyunsaturated fatty acid oil sunflower seed oil as a core material, and the preparation process parameters of oil microcapsules were optimized by single factor experiment and response surface experiment. Results: The best technological conditions of oil microcapsule were solid content of 25.2%, and the mass ratio of composite wall material β-cyclodextrin: gelatin was 6.7∶1. The dosage of emulsifier was 1%, and the mass ratio of core wall material was 1∶2. Under this condition, the prepared oil microcapsule particles were round. The particle size was uniform, and the embedding rate was 94.33%. The content of polyunsaturated fatty acid was 21.73%. Conclusion: This preparation method is feasible and can be used to prepare high concentration polyunsaturated fatty acid oil microcapsules.

【基金】 国家自然科学基金面上项目(编号:81871414);湖北省教育厅科研计划项目(编号:B2021294);武汉东湖学院2021年“东湖未来之星”大学生科研重点项目(编号:3)
  • 【文献出处】 食品与机械 ,Food & Machinery , 编辑部邮箱 ,2022年08期
  • 【分类号】TS221
  • 【下载频次】236
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