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湿法消解-火焰原子吸收光谱法测定富硒农产品中的硒
Determination of Selenium in Selenium-rich Agricultural Products by Atomic Absorption Spectrometry
【摘要】 建立湿法消解-火焰原子吸收光谱法测定富硒农产品中硒元素质量浓度的方法。采用硝酸-高氯酸(4:1)对样品进行消解处理,利用原子吸收光谱仪进行检测。结果表明,在 2.0~12.0 μg·L-1质量浓度范围内,吸收强度与浓度呈良好的线性关系,回归方程为 y=0.009 2x+0.010 6,r=0.999 3。该方法操作简便,结果准确,适用于农产品中硒的质量浓度分析。
【Abstract】 A determination method of selenium in selenium-rich agricultural products by atomic absorption spectrometry with wet digestion was established. The samples were pretreated with nitric acid-perchloric acid (4∶1), and were determined by AAS. The results showed that the linear regression equation of selenium was y = 0.009 2x + 0.010 6 in the range of 2.0~ 12.0 μg·L-1, r=0.999 3.The method was simple, accurate and suitable for the analysis of selenium in agricultural products.
【基金】 辽宁省教育厅科学研究项目(项目编号:SYSF202012);大学生创新训练项目(项目编号:202110169027)资助
- 【文献出处】 辽宁化工 ,Liaoning Chemical Industry , 编辑部邮箱 ,2022年11期
- 【分类号】O657.31;TS207.3
- 【下载频次】85