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N-磺酰基Pictet-Spengder反应制备1-苯基异喹啉的合成研究
Study on the synthesis of 1-Phenylisoquinoline
【摘要】 1-苯基异喹啉具有刚性结构和较大的共轭体系,可以使发射光谱产生红移以提高红发光纯度,是OLED磷光染料的优良配体。使用苯乙胺和苯甲醛为原料,经N-磺酰基P-S三步反应制备出1-苯基异喹啉,结果表明其纯度可达到98.5%。
【Abstract】 1-phenylisoquinoline has a rigid structure and a large conjugate system, which can make the emission spectrum red-shift and improve the red luminescence purity. 1-phenylisoquinoline was prepared by N-sulfonyl P-S three-step reaction using phenylethylamine and benzaldehyde as raw materials and the purity of the product reaches 98.5%.
- 【文献出处】 信息记录材料 ,Information Recording Materials , 编辑部邮箱 ,2022年10期
- 【分类号】O626.323
- 【下载频次】8