【摘要】 本文以邻叔丁基苯酚为起始原料,经溴化、偶连和甲酰化三步反应制得联苯型双水杨醛化合物,再与2,6-二甲基苯胺发生席夫碱反应得到双水杨醛亚胺型席夫碱配体,探讨了合成条件对制备过程的影响并通过1H NMR、13C NMR和FT-IR等手段对所得化合物进行表征。更多还原

【Abstract】 In this paper,the biphenylsalicylaldehyde compound was synthesized with o-tert-butylphenolas the starting material through three steps including bromination,coupling and formylation,which then reacted with 2,6-dimethylaniline bythe Schiff basereaction to obtain biphenyl salicylaldiminebidentate Schiff base ligand. The influence of reaction conditions on the preparation process were discussed. The obtained compounds were characterized by 1H NMR,13 C NMR and FT-IR.更多还原