节点文献
一例新颖的三维铜基配位聚合物的合成及结构表征
Synthesis and Structural Characterization of a Novel 3D Copper(Ⅱ) Coordination Polymer
【摘要】 本文首先合成了4-(2-(4-吡啶基)乙烯基)苯甲酸有机配体,进而与Cu(NO3)2·3H2O在溶剂热的反应条件下,合成了一例新颖的三维铜的配位聚合物{[Cu(pyeb)2]·DMF}n(1),通过单晶/粉末X-射线衍射、红外光谱对其结构进行了表征。
【Abstract】 In this paper, firstly, bis{4-[2-(4-pyridyl)ethenyl] benzoic acid ligand was synthesized, and then a novel three-dimensional copper coordination polymer {[Cu(pyeb)2]·DMF}n(1) was synthesized with Cu(NO3)2·3H2 O under solvothermal method. The structure of compound 1 was characterized by single crystal/powder X-ray diffraction and infrared spectroscopy.
【基金】 结构化学国家重点实验室开放基金(20180030);国家自然科学基金(21801071,21902046);湖北省科技厅基金(2018CFB171)
- 【文献出处】 胶体与聚合物 ,Chinese Journal of Colloid & Polymer , 编辑部邮箱 ,2020年03期
- 【分类号】O641.4
- 【下载频次】140