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6-姜烯酚的NMR数据解析
An NMR Study on 6-Shogaol
【摘要】 用NMR数据解析方法对姜辣素类化合物6-姜烯酚[6-Shogaol,(E)-1-(4-羟基-3-甲氧基苯基)癸-4-烯-3-酮]的结构进行研究.联合应用一维NMR(1H NMR、13C NMR、DEPT)和二维NMR(1H-1H COSY、HSQC、HMBC)技术对其进行检测,使6-姜烯酚所有的1H和13C NMR数据得到了详细解析和归属,并进一步确证其结构.本研究为姜辣素类化合物的结构鉴定提供了可靠的NMR数据解析方法和依据,也为该类化合物的深入研究提供了结构信息.
【Abstract】 The structure of 6-Shogaol[(E)-1-(4-Hydroxy-3-methoxy-phenyl)dec-4-en-3-one]was studied by NMR data analysis method and was detected by 1 D NMR(1 H NMR,13 C NMR and DEPT)and 2 D NMR(1 H-1 H COSY,HSQC and HMBC)techniques. The results show that the 1 H and 13 C NMR spectra are analyzed and assigned,and the structures of 6-Shogaol are further identified. This research provided not only NMR data analysis methods and evidences,but also structures information for the structures identification of Gingerols.
【Key words】 NMR; assignment; ~1H-~1H COSY; HSQC; HMBC; 6-Shogaol;
- 【文献出处】 河南科学 ,Henan Science , 编辑部邮箱 ,2020年05期
- 【分类号】O657.2;TQ28
- 【下载频次】106