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爆炸喷涂铁基非晶涂层的微观结构和纳米压痕行为

Microstructure and nano-indentation behavior of detonation sprayed iron-based amorphous coating

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【作者】 欧阳晟储志强唐求豪解路

【Author】 OUYANG Sheng;CHU Zhiqiang;TANG Qiuhao;XIE Lu;Hunan Metallurgy Material Institute Co., Ltd.;Hunan Provincial Key Laboratory of Advanced Materials for New Energy Storage and Conversion,Hunan University of Science and Technology;State Key Laboratory of Powder Metallurgy, Central South University;

【通讯作者】 欧阳晟;

【机构】 湖南省冶金材料研究院有限责任公司湖南科技大学新能源储存与转换先进材料湖南省重点实验室中南大学粉末冶金国家重点实验室

【摘要】 采用爆炸喷涂在3种不同氧燃比的条件下制备铁基非晶涂层,采用X射线衍射(XRD)仪、扫描电镜、纳米压痕仪等研究涂层的微观结构和纳米压痕行为。结果表明:氧燃比为1:1、1.2:1和1.5:1的3种涂层的非晶含量分别为88.71%、86.18%和81.36%。压痕深度在不同载荷下均表现出相似的变化速率,意味着涂层微观结构的高度均匀性。在相似打点位置,氧燃比为1:1和1.2:1的涂层具有较高的硬度,显示出较小的最大压痕深度。在平行于涂层与基体界面方向,纳米硬度几乎无变化,而在垂直于界面方向,随涂层厚度增加,纳米硬度从16.75 GPa降低至10.25 GPa。

【Abstract】 The iron-based amorphous coatings were prepared by detonation spray under three kinds of oxygen fuel ratios. The microstructure and nanoindentation behavior were examined by XRD, SEM and nanoindenter. The results show that the amorphous phase contents of coatings under 1:1, 1.2:1 and 1.5:1 are calculated to be 88.71%, 86.18% and 81.36%, respectively. The variation speeds of indentation depth are similar under different load, indicating the homogenous coating structure. In similar position, the coatings under oxygen fuel ratios of 1:1 and 1.2:1 have higher hardness, exhibiting smaller maximum indentation depth. In the longitudinal direction, the variation of nanohardness is very small. In the transverse direction, the nanohardness value decreases from 16.75 GPa to 10.25 GPa with increasing the distance from the coating to the substrate.

【基金】 高端轴承摩擦学技术与应用国家地方联合工程实验室(河南科技大学)开放基金(201913);材料表界面科学与技术湖南省重点实验室(中南林业科技大学)开放基金(KFBJM2019002)
  • 【文献出处】 粉末冶金材料科学与工程 ,Materials Science and Engineering of Powder Metallurgy , 编辑部邮箱 ,2020年06期
  • 【分类号】TG174.4
  • 【被引频次】2
  • 【下载频次】288
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