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超细晶粉末冶金CoCrFeMnNiGd0.15高熵合金的组织性能
Microstructure and Mechanical Properties of Ultrafine-Grained CoCrFeMnNiGd0.15 High-Entropy Alloy Fabricated by Powder Metallurgy
【摘要】 采用机械合金化和放电等离子烧结的方法制备出超细晶CoCrFeMnNiGd0.15合金,研究了CoCrFeMnNiGd0.15高熵合金的组织与性能。结果表明,其组织为多相结构,基体为fcc固溶体相,析出相为稀土氧化物(Gd2O3)和富Gd、Ni、Mn的四方结构相。随着烧结温度的提高,析出相的含量不断增加且尺寸不断增大,合金的压缩屈服强度不断下降而塑性则不断上升。在900℃烧结时材料具有最优的综合力学性能,其压缩屈服强度(σ0.2)、抗压强度(σmax)、断裂时的塑性应变(εp)和维氏硬度分别达到1662 MPa、2518 MPa、30.6%和4580 MPa。
【Abstract】 The ultrafine-grained CoCrFeMnNiGd0.15 high-entropy alloy(HEA) was prepared by mechanical alloying(MA) and spark plasma sintering(SPS).The microstructure and mechanical properties of CoCrFeMnNiGd0.15 high-entropy alloy were investigated.Results indicate that the sintered CoCrFeMnNiGd0.15 alloy shows a multi-phase microstructure including the fcc matrix, a rare earth oxide(Gd2O3) and a tetragonal phase rich in Gd, Ni and Mn element.As the sintering temperature increases, the content and size of the precipitated phase increase continuously, the compressive yield strength of the alloy decreases while the plasticity shows the opposite trend.The sintered alloy achieves the best comprehensive mechanical properties at the sintering temperature of 900 ℃, with compressive yield strength of 1662 MPa, compressive strength of 2518 MPa, plastic strain of 30.6 % and Vickers hardness of 4580 MPa.
【Key words】 metallic materials; high-entropy alloys; powder metallurgy; rare earth element Gd; microstructure; mechanical properties;
- 【文献出处】 稀有金属材料与工程 ,Rare Metal Materials and Engineering , 编辑部邮箱 ,2020年11期
- 【分类号】TG139
- 【被引频次】6
- 【下载频次】230