节点文献

喷雾干燥法制备RGO/Cu复合粉体及其复合材料性能研究

Renforced mechanical properties of reduced graphene oxide/copper composites using spray drying

  • 推荐 CAJ下载
  • PDF下载
  • 不支持迅雷等下载工具,请取消加速工具后下载。

【作者】 熊轶娜胡柏新陈小华许龙山

【Author】 XIONG Yi-na;HU Bai-xin;CHEN Xiao-hua;XU Long-shan;Changsha Aeronautical Vocational Technical College;College of Materials Science and Engineering,Hunan University;College of Materials Science and Engineering,Xiamen University of Technology;

【通讯作者】 陈小华;

【机构】 长沙航空职业技术学院湖南大学材料科学与工程学院厦门理工学院材料科学与工程学院

【摘要】 以铜盐和氧化石墨烯(GO)为原料,采用喷雾干燥-煅烧-还原工艺获得了超细RGO/Cu复合粉体,X射线衍射(XRD)和扫描电镜(SEM)结果表明,复合粉体纯度高,粒径细小,RGO分散均匀。利用快速等离子体烧结工艺(SPS)和模压成型(MP)制备出不同含量RGO/Cu复合材料,对两种样品的微观结构、硬度和导电性能进行研究,结果显示,SPS工艺远优于MP成型烧结工艺,RGO含量为3wt%时,复合材料综合性能最佳。SPS工艺制备样品显微硬度(164.45HV)相比于同工艺下纯铜硬度值提高了32.36%,电导率达87.51%IACS。

【Abstract】 Reduced graphene oxide(RGO)/Cu ultrafine powders were fabricated by copper salt and graphene oxide(GO)via spraying drying-calcination-hydrogen reduction method. The results of X-ray diffraction(XRD)and scanning electron microscopy show that the powders have high purity,small particle size and RGO homogeneous distribution.The RGO/Cu composites with different content were prepared by mould pressing(MP)and spark plasma sintering(SPS).The microhardness,eletrical conductivity and microstructure of RGO/Cu composites were researched.The results display that SPS was superior to MP,and the composite with 3 wt%RGO obtained by SPS can achieved 87.51%IACS in eletrical conductivity and had a 32.36%improvement in hardness compared with Cu.

【基金】 国家自然科学基金项目(51272073,51154001)资助;湖南省自然科学基金科教联合项目(2018JJ5059)资助
  • 【文献出处】 化学研究与应用 ,Chemical Research and Application , 编辑部邮箱 ,2019年04期
  • 【分类号】TB33
  • 【下载频次】142
节点文献中: 

本文链接的文献网络图示:

本文的引文网络