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双连续Si3N4/1Cr18Ni9Ti复合材料的制备和冲蚀性能

Preparation and Erosion Performance for Co-continuous Phase Composites of Si3N4/1Cr18Ni9Ti

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【作者】 杜奇高勇任志恒曹小明王超张劲松

【Author】 DU Qi;GAO Yong;REN Zhiheng;CAO Xiaoming;WANG Chao;ZHANG Jinsong;Institute of Metal Research,Chinese Academy of Science;School of Materials Science and Engineering,University of Science and Technology of China;Liaoning ZhuoYi New Materials Corporation;

【通讯作者】 张劲松;

【机构】 中国科学院金属研究所中国科学技术大学材料科学与工程学院辽宁卓异新材料有限公司

【摘要】 用凝胶注模和压力铸造两步法制备具有双连续结构的Si3N4/1Cr18Ni9Ti复合材料并分析其物相组成、宏观和微观结构,研究了材料的冲蚀率与攻角、流速、含沙量以及时间的关系。结果表明,与1Cr18Ni9Ti材料相比,Si3N4/1Cr18Ni9Ti复合材料具有双连续结构,界面结合良好;其冲蚀率随着攻角变化的幅度小,冲蚀率与流速之间的关系由1Cr18Ni9Ti材料的线性关系转变为指数关系(E∝V0.67),且随着时间的延长冲蚀率降低;冲蚀率与含沙量之间的关系仍呈线性。具有双连续结构的Si3N4/1Cr18Ni9Ti复合材料,具有更加优异的耐冲蚀性能。

【Abstract】 Composites with co-continuous structure of Si3N4/1Cr18Ni9 Ti were prepared via a twostep process, namely gel casting and pressure casting. The phase composition, macro-and micro-structure of the composites were characterized. The erosion rate in flow slurry composed of water and quartz sand, as a function of impingement angle, flow velocity, sand content and erosion time was assessed in comparison with the plain 1Cr18Ni9 Ti. Results show that Si3N4/1Cr18Ni9 Ti composites exhibited a perfect co-continuous phase structure with a good combination between Si3N4 and 1Cr18Ni9Ti; the fluctuation of erosion rate as a function of impingement angle of this composites is smaller than that of 1Cr18Ni9Ti; the erosion rate of composites has an exponent relationship with flow velocity(E∝V0.67), while there is a linear relationship between the erosion rate and flow velocity for 1Cr18Ni9Ti; the erosion rate of this composites decreases gradually with the increasing erosion time and then stabilizes, while that of 1Cr18Ni9 Ti is hardly changed; There is a linear relationship between the erosion rate and sand content in the slurry for the two materials. The composite with co-continuous structure of Si3N4/1Cr18Ni9 Ti exhibits superior erosion resistance, in contrast with the plain 1Cr18Ni9 Ti steel.

【基金】 国家重点研发计划重点专项(2017YFB0310405)~~
  • 【文献出处】 材料研究学报 ,Chinese Journal of Materials Research , 编辑部邮箱 ,2019年01期
  • 【分类号】TB33
  • 【被引频次】4
  • 【下载频次】134
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