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新型时效热处理工艺对多芯NbTi超导线材微观组织和临界电流密度的影响

Effect of New Heat Treatment on Microstructure and Critical Current Density of NbTi Superconducting Wire

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【作者】 郭强张平祥冯勇刘向宏李建峰闫凯鹃

【Author】 Guo Qiang;Zhang Pingxiang;Feng Yong;Liu Xianghong;Li Jianfeng;Yan Kaijuan;Western Superconducting Technologies Co.Ltd;National Engineering Laboratory for Superconducting Materials;Northwest Institute for Nonferrous Metal Research;

【通讯作者】 郭强;

【机构】 西部超导材料科技股份有限公司超导材料制备国家工程实验室西北有色金属研究院

【摘要】 以高均匀性Nb47Ti合金棒和高纯无氧铜为原材料,制备了铜比1.3,630芯的NbTi/Cu超导线。提出了一种新型时效热处理工艺"短时预时效热处理+高温长时间时效热处理",即"405℃/3 h+405℃/3 h+420℃/20 h+420℃/40h+420℃/80h"工艺,该工艺可显著提高NbTi超导线材的临界电流密度,较普通热处理线材提高近17.5%,最高可以达到3208A/mm~2。足够的预时效次数(2次)才能使基体中析出足够多的α形核数量,进而才能在较大的最终应变下显著提高临界电流密度。此外,在4.46,5.35,6.25 3种预应变条件之下,临界电流密度达到峰值的最终应变都集中在5.0~5.2之间,即,必须将最终应变控制在5.0~5.2。

【Abstract】 NbTi/Cu wire with the low copper-to-superconductor ratio of 1.3 and filament number of 630 was prepared using highly homogenous Nb47 Ti alloy bar and oxygen-free copper. A new type of aging heat treatment(405 °C/3 h+405 °C/3 h+420 °C/20 h+420 °C/40 h+420 °C/80 h) was proposed. Compared with the traditional heat treatment, this new type heat treatment can largely improve the critical current density of NbTi superconducting wire to 3208 A/mm2, with an increment of 17.5%. When the pre-heat treatment times are equal to or more than 2 times, enough nucleation can be formed and critical current density can be improved obviously. In addition, critical current densities of wire under three pre-strain conditions(4.46, 5.35 and 6.25) all get the peak value when final strain is between 5.0~5.2. So, the pre-strain should be controlled between 5.0~5.2.

【基金】 陕西省国际科技合作计划项目(2017KW-022)
  • 【文献出处】 稀有金属材料与工程 ,Rare Metal Materials and Engineering , 编辑部邮箱 ,2019年12期
  • 【分类号】TM26
  • 【被引频次】3
  • 【下载频次】187
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