【摘要】 利用溶剂热合成法制备金属有机骨架材料MIL-53(Fe)。通过X射线衍射仪(XRD)、电子扫描电镜(SEM)、傅立叶变换红外光谱仪(FTIR)表征手段对材料的晶相结构及组成成分进行分析。常温常压下,通过催化还原对硝基苯酚的反应考察MIL-53(Fe)的催化活性。结果表明,MIL-53(Fe)的催化活性良好,5min对硝基苯酚的转化率达到96.8%。更多还原

【Abstract】 In this paper,MIL-53(Fe)was prepared by sol-thermal method.The structure and composition of sample was characterized by means of X-ray diffraction(XRD),scanning electron microscopy(SEM),Fourier transformation infrared spectrometer(FTIR).Catalytic activity of sample was investigated by catalytic reduction of p-nitrophenol at ambient temperature and pressure.The results showed that MIL-53(Fe)existed good catalytic performance and the conversion of p-nitrophenol reached96.8%in five minutes.更多还原