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激光预处理对HfO2光学薄膜微观性能的影响

Influence mechanism of laser conditioning on the microcosmic properties of HfO2 optical thin films

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【作者】 杨利红薛鹏成王涛苏俊宏

【Author】 YANG Li-hong;XUE Peng-cheng;WANG Tao;SU Jun-hong;Shool of Optoelectronics Engineering,Xi′an Technological University;Xi′an Institute of Optics and Precision Mechanics,Chinese Academy of Sciences;

【机构】 西安工业大学光电工程学院中国科学院西安光学精密机械研究所

【摘要】 研究了在1-on-1方式下激光预处理对HfO2光学薄膜微观形貌、微观结构等性能的影响。实验采用薄膜阈值能量的10%、30%、50%和70%对HfO2薄膜进行激光预处理,利用原子力显微镜(AFM)分别对预处理后薄膜表面10μm×10μm和3μm×3μm的区域进行测试,与预处理前相比,预处理后的薄膜所含杂质减少,薄膜表面锥状结构变得平滑;利用X射线衍射(XRD)和X射线光电子能谱(XPS)分别对预处理后薄膜的晶态结构和化学键以及价态进行测试,与预处理前相比,预处理后薄膜的晶态结构、化学键及价态均没有发生变化;利用XPS对预处理后薄膜所含的成分进行测试,与预处理前相比,预处理后薄膜中所含的Hf单质减少,HfO2增多。实验结果表明,激光预处理具有抛光和氧化膜层的作用。

【Abstract】 In 1-on-1 case the influence of laser conditioning on the microscopic morphology and structure of HfO2 optical thin film is studied.The HfO2 thin films were irradiated with 10%,30%,50%and 70%of the threshold energy in 1-on-1.In order to research the microscopic morphology of HfO2 optical thin film,the film surface areas of 10μm×10μm and 3μm×3μm were tested with atomic force microscope.Comparing laser conditioning with non-laser conditioning,the thin film being irradiated contains less impurities and its cone-shaped structure becomes smooth.The microscopic structure of thin film was tested with X-ray diffraction and X-ray photoelectron spectroscopy.Comparing laser conditioning with non-laser conditioning,the crystalline structure,the chemical bond and the element valence of thin film being irradiated are not changed.The components of thin film were tested with X-ray photoelectron spectroscopy.Comparing laser conditioning with non-laser conditioning,the thin film being irradiated contains less hafnium and more oxides of hafnium.The experimental results show that the laser conditioning plays an important role in polishing and oxidizing HfO2 thin film.

【关键词】 薄膜抛光激光预处理HfO2氧化
【Key words】 thin filmpolishinglaser conditioningHfO2oxidizing
【基金】 国家自然科学基金(61378050);陕西省自然科学基金(2016JZ025);陕西省国际科技合作(2016kw-036)资助项目
  • 【文献出处】 光电子·激光 ,Journal of Optoelectronics·Laser , 编辑部邮箱 ,2018年02期
  • 【分类号】TB383.2;TN249
  • 【被引频次】2
  • 【下载频次】211
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