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石墨烯/Fe2(MoO4)3复合物的制备与电化学特性研究
Preparation and Electrochemical Properties of Fe2(MoO4)3/Graphene Composite Materials
【摘要】 首先通过Hummers法制备氧化石墨烯,然后石墨烯为模板用水热法将其与Fe2(MoO4)3复合,成功制备了石墨烯/Fe2(MoO4)3三维多孔复合物。通过XRD、扫描电镜、拉曼光谱以及红外光谱对制备的石墨烯/Fe2(MoO4)3复合物进行结构和形貌表征,并测试了其电化学特性。结果显示石墨烯/Fe2(MoO4)3复合物呈多孔结构,且Fe2(MoO4)3颗粒分散在石墨烯孔隙间,循环伏安曲线显示复合物有优良的电化学性能。
【Abstract】 The graphene was prepared through using graphite as raw material by Hummers,and then it was combined with Fe2(MoO4)3 with using hydrothermal method to obtain the different ratio of Fe2(MoO4)3/graphene complex. Finally,the structure and morphology of the prepared graphene/Fe2(MoO4)3 complex were characterized by Raman spectroscopy,XRD,sem and so on.The results show that the structure and morphology of Fe2(MoO4)3/graphene complex are basically in line with the test requirements,and also show that electrochemical properties are very good.
【Key words】 Fe2(MoO4)3; rGO; thermal reaction of water; electrochemical analysis of chemical; Raman spectroscopy; IR; XRD; scanning electron microscope;
- 【文献出处】 大学物理实验 ,Physical Experiment of College , 编辑部邮箱 ,2018年05期
- 【分类号】TB332
- 【被引频次】2
- 【下载频次】180