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β-CEZ钛合金在固溶时效时ω相与α相的组织演化规律

Microstructure Evolution of ω and α Phase of β-CEZ Alloy During the Solution Treatment and Aging Process

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【作者】 何涛冯勇刘向宏罗文忠田琳何永胜

【Author】 He Tao;Feng Yong;Liu Xianghong;Luo Wenzhong;Tian Lin;He Yongsheng;State Key Laboratory of Solidification Processing,Northwestern Polytechnical University;NLEL for Special Titanium Alloy Material Manufacturing,Western Superconducting Technology Co.,Ltd;

【机构】 西北工业大学凝固技术国家重点实验室西部超导材料科技股份有限公司特种钛合金材料制备技术国家地方联合工程实验室

【摘要】 主要通过SEM和TEM观察固溶时效过程β-CEZ钛合金ω相和α相的组织变化规律。发现β-CEZ合金在固溶处理后析出尺寸1~2 nm的无热ω相,在350~500℃时效处理时,ω相辅助形核析出长100~200 nm的针状α相,且随着时效温度升高,α相数量增多,尺寸略有长大。当时效温度达到550℃时,ω相基本消失,α相继续长大到约300nm。当时效温度升高到650℃以后,晶界析出大量的长条状α相,晶内α相长度长大到数微米。

【Abstract】 The microstructure evolution of ω and α phase in the solution treatment and aging process of β-CEZ alloy,which is a kind of typical near-β titanium alloy,was researched.The results show that ultrafine athermal ω precipitates(about 1~2 nm) are formed in β-CEZ alloy by quenching above the β transus temperature.Needle-like α precipitates,about 100 nm in length,are formed when solution treated β-CEZ alloy samples are aged at 350 ℃.The ω assisted α increases to about 200 nm in length while increasing ageing temperature to 500 ℃.The α precipitates grow to about 300 nm in length and ω disappears when the ageing temperature increases to 550 ℃.Long strip shape α is formed at grain boundaries and the intragranular α increases to several microns in length when the β-CEZ alloy samples are aged above 650 ℃.

【关键词】 β-CEZ固溶时效ω相α相组织变化
【Key words】 β-CEZsolution and agingω phaseα phasemicrostructure evolution
【基金】 国家国际科技合作专项(2013DFR50090);陕西省重大科技成果转化引导专项(2015KTCG01-11)
  • 【文献出处】 稀有金属材料与工程 ,Rare Metal Materials and Engineering , 编辑部邮箱 ,2018年09期
  • 【分类号】TG146.23
  • 【被引频次】4
  • 【下载频次】179
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