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丙三醇液相插层制备优级煤系高岭土
Preparation of Premium Grade Coal Kaolin by Liquid-phase Intercalation with Glycerol
【摘要】 以大颗粒的煤系高岭土矿为原料,丙三醇为插层剂,通过插层空化工艺、湿法球磨、喷雾干燥制备优级高岭土。通描电子显微镜(SEM)、能谱仪(EDS)、X射线衍射(XRD)等对煤系高岭土产品的微观形貌结构和成份进行分析,采用白度仪测定样品白度。结果显示,所得样品晶态好、白度高、细度小、纯度高、颗粒分布均匀,远高于优级高岭土的要求。
【Abstract】 The kaolinite was prepared through the intercalation cavitation process, wet ball-milling,spray dryingusing the large particles of coal-based kaolinore as raw material and glycerol as intercalation agent.The microstruc-ture and composition of coal kaolin products were analyzed by electron microscopy(SEM), energy dispersive spec-trometer(EDS)and X-ray diffraction(XRD).The shiteness of the sample was measured by a whiteness, small fine-ness, high purity and uniform distrbution of particles, which much higher than of gorden gade.
【关键词】 煤系高岭土;
丙三醇;
插层空化法;
湿法球磨;
喷雾干燥;
【Key words】 coal kaolin; propanetriol; intercalation caviation; wet ball-milling; spray dry;
【Key words】 coal kaolin; propanetriol; intercalation caviation; wet ball-milling; spray dry;
【基金】 山西大同大学校级青年科研项目经费[2015Q7];大同市科技公关项目[2015Q24]
- 【文献出处】 山西大同大学学报(自然科学版) ,Journal of Shanxi Datong University(Natural Science Edition) , 编辑部邮箱 ,2017年02期
- 【分类号】TD985
- 【下载频次】88