In this study,the separation models of o-vanillin and vanillin with three-zone simulated moving bed(SMB)and Varicol were built.The separation of these two compounds was achieved successfully with high efficiency and high purity in the experiment.Firstly,the mobile phase of 35%(by vol.)aqueous alcohol and the stationary phase of reverse phase C18 silica gel were determined.The adsorption isotherms of these two compounds were determined with single-component frontal analysis.The lumped mass transfer coefficie...
【基金】
厦门市科技计划项目(3502Z20143008)
【更新日期】
2017-08-11
【分类号】
TQ028;TQ655
【正文快照】
492-498.Citation:CHEN J L,YAO C Y,LU Y H.Three-zone simulated moving bed for separation of o-vanillin and vanillin[J].J XiamenUniv Nat Sci,2017,56(4):492-498.(in Chinese)香兰素(3-甲氧基-4-羟基苯甲醛)是一种广泛应用于食品添加剂、日用化学品、医药中间体、精细