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效应面法优选甜茶素提取工艺

Optimization of Extraction Process of Rubusoside by Response Surface Method

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【作者】 吴婕吴超宫江宁廖莉玲

【Author】 WU Jie;WU Chao;GONG Jiang-ning;LIAO Li-ling;College of Chemistry and Life Science, Guizhou Normal College;School of Chemistry and Material Science, Guizhou Normal University;

【机构】 贵州师范学院化学与生命科学学院贵州师范大学化学与材料科学学院

【摘要】 为了甜茶素的工业化生产,在甜茶叶中提取甜茶素的单因素试验基础上,采用效应面法优选出甜茶素的提取工艺参数,建立关于甜茶素提取率的二项式拟合方程,得到的最佳提取工艺参数:乙醇体积分数54.45%,提取温度70.21℃,液料比15.13 m L/g,提取时间2.1 h,甜茶素提取率的预测值3.615 3%。同时为了检验此工艺条件在实际工业生产中的可靠性,改进工艺条件为:提取温度70℃,乙醇体积分数55%,提取时间2.0 h,液料比15 m L/g,得到甜茶素提取率的实际值与其二项式拟合方程的预测值偏差仅为1.24%。故效应面法优选出的甜茶素的提取工艺参数,方法简便、可靠。

【Abstract】 Based on the single factor test of extraction rubusoside, response was used to explore the optimum extraction parameters of rubusoside for industry. The rubusoside extraction regression equation was established and the optimal extraction processing parameters were determined. The optimal conditions of extraction process were followed: extraction temperature of 70.21 ℃, ethanol concentration of 54.45 %, extraction time of 2.1 h and liquid-material ratio of 15.13 m L/g. Under this condition, the rubusoside extraction rate was 3.615 3 %. In order to test the reliability of the process condition in industry, the best verification processing parameters were followed: extraction temperature of 70 ℃, ethanol concentration of 55 %, extraction time of 2.0 h and liquidmaterial ratio of 15 m L/g. The variance between the result of the best verification test and the binomial fitting equation forecast value was nearly 1.24 %. Thus, The optimized extraction parameters were simple and reliable.

【关键词】 甜茶提取工艺甜茶素效应面法
【Key words】 sweet teaextraction technologyrubusosideresponse method
  • 【文献出处】 食品研究与开发 ,Food Research and Development , 编辑部邮箱 ,2017年11期
  • 【分类号】TS202.3
  • 【被引频次】2
  • 【下载频次】186
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