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泌感合剂的质量标准提高研究
Study on the Quality Standard of Mi-gan Mixture
【摘要】 目的提高泌感合剂的质量标准。方法通过薄层色谱法鉴别地榆和土茯苓;通过AlCl3络合法,采用紫外分光光度法测定泌感合剂中总黄酮的含量。结果总黄酮在0.044 40.133 3 mg范围内具有良好的线性关系,线性方程为Y=46.57X-0.001,r=0.999 8,平均回收率为92.85%,RSD为1.77%(n=6)。结论该方法简单、准确、数据可靠,可作为泌感合剂的质量控制方法。
【Abstract】 Objective To improve the quality standard of Mi-gan Mixture. Methods The Sanguisorba officinalis and Smilacis Glabrae Rhizoma are identified by thin layer chromatography.The content of total flavonoids is determined by UV spectrophotometry by AlCl3 complexation method. Results The total flavonoids have a good liner in the range of 0.044 4 0.133 3 mg, the linear equation is Y = 46.57 X-0.001, r = 0.999 8,the average recovery is 92.85 % and the RSD is 1.77 %(n = 6). Conclusion The method is simple and accurate, which can be used as the quality control method of Mi-gan Mixture.
【Key words】 Mi-gan mixture; Sanguisorba officinalis; Smilacis Glabrae Rhizoma; total flavonoids; quantitative method;
- 【文献出处】 现代中药研究与实践 ,Research and Practice on Chinese Medicines , 编辑部邮箱 ,2017年06期
- 【分类号】R286.0
- 【被引频次】2
- 【下载频次】172