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脉冲激光沉积低内应力多层类金刚石膜
Multilayer-DLC film with low inner-stress prepared by pulsed laser deposition
【摘要】 为解决类金刚石膜内应力极大的问题,利用很薄的岛状结构锗层与较厚的类金刚石层循环,设计并制备了具有低内应力的多层类金刚石膜。其中,类金刚石层为主要功能膜层,起到硬质保护和光学增透的作用;而锗层作为缓冲层,起到缓解纯类金刚石膜内应力过大的问题,同时由于锗层很薄,对整个膜层的机械性能和红外特性的影响很小。测试表明,制备的多层类金刚石膜内应力为2.14 GPa,比纯类金刚石膜降低了39%,通过了GJB2485-95《光学膜层通用规范》中的重摩擦测试;同时,其纳米硬度仍保持在47 GPa的高水平。该多层类金刚石膜可以作为实际应用的红外窗口保护膜。
【Abstract】 Multilayers diamond-like carbon film,which was composed of several thick diamond-like carbon layers and thin germanium island layers,was prepared on the germanium substrate in order to resolve the high inner-stress in the diamond-like carbon film.The diamond-like carbon layers had the main function of protection,and the germanium island layers had the buffer function to reduce the inner-stress in the diamond-like carbon film.Meanwhile,the thicknesses of the germanium layers were very thin,so they had no influence on the mechanical and infrared performances of the whole film nearly.Inner-stress in the multilayers diamond-like carbon film was 2.14 GPa,39% lower than that of the pure diamond-like carbon film,and the multilayers diamond-like carbon film could pass the friction test stipulated in the GJB2485-95 ′ general specification for optical coatings.The hardness of the multilayers diamond-like carbon kept high hardness of 47 GPa,and had the same surface roughness to the pure diamond-like carbon film.Therefore,the multilayers diamond-like carbon film could be used as practical protective film for infrared window.
【Key words】 pulsed laser deposition; multilayers diamond-like carbon film; germanium buffer layers; low inner-stress;
- 【文献出处】 红外与激光工程 ,Infrared and Laser Engineering , 编辑部邮箱 ,2017年09期
- 【分类号】TB383.2;TQ163
- 【被引频次】2
- 【下载频次】110