Fifteen kinds of PAEs in water were determined by gas chromatography with solid-phase extraction in this research. The optimal conditions of pretreatment were discussed. The results indicated that the linearity was good from 0. 500 mg/L to 20. 0 mg/L. The detection limits were from 0. 20 μg/L to 0. 39 μg/L. The spiked recoveries of blank water samples were 66. 6% ~ 120%,and the relative standard deviations of 6 repeated measurements were 5. 7% ~ 12. 5%. The spiked recoveries of actual water samples were 66....