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胺唑草酮原药的高效液相色谱分析

Analysis Method of Amicarbazone Technical by HPLC

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【作者】 李璇兆奇武铁军王玉范唐霞

【Author】 LI Xuan;Zhao Qi;Wu Tiejun;Wang Yufan;Tang Xia;Shenyang Research Institute of Chemical Industry Co., Ltd.;

【机构】 沈阳化工研究院有限公司

【摘要】 [目的]建立了胺唑草酮的高效液相色谱分析方法,采用Waters Symmetry?C18色谱柱,紫外可变波长检测器,检测波长223nm;以乙腈-水(体积比60:40)为流动相,流速0.8m L/min。外标法对主要成分进行定量分析,在0.250.0mg/L范围内线性相关系数为0.9999,平均回收率为99.099.2%,样品测定的相对标准偏差0.5%。

【Abstract】 A method was established for analyzing Amicarbazone by HPLC using the Waters Symmetry? C18 column and a variable wavelength UV detector at 223 nm, the mobile phase was a mixture of acetonitrile and water(60:40, by vol) at a flow rate of0.8ml/min. Quantitative analysis of effective ingredients was carried out using external standard method. The results demonstrated that the linearity correlation coefficient was 0.9999 in the range of0.2mg/L to 50.0mg/L, the average recovery was 99.099.2%, the variation coefficient was 0.3%.

【关键词】 胺唑草酮除草剂高效液相色谱
【Key words】 AmicarbazoneherbicideHPLC
  • 【文献出处】 化工管理 ,Chemical Enterprise Management , 编辑部邮箱 ,2017年21期
  • 【分类号】O657.72;TQ457.2
  • 【被引频次】1
  • 【下载频次】60
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