An efficient and practical palladium-catalyzed cascade oxidative heterocyclization has been developed to afford functionalized oxygen-containing five-membered heterocycles in moderate to good yields with high regio-and diastereoselectivities.Their structures were confirmed by IR,~1H NMR,~(13)C NMR and HRMS.Furthermore,the current methodology could also be conveniently applied to the synthesis of naturally occurring biologically active functionalized tetrahydrofurans and γ-lactones frameworks.
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