Copper hydroxyphosphate(Cu2(OH)PO4) was quickly synthesized by microwave-assisted method at low temperature(< 100℃) and normal atmosphere pressure, then characterized by XRD, SEM and Raman spectra. The synthesis parameters were investigated by a series of controled experiments. It is found that molar ratio, initial concentration of Cu Cl2 and Na H2PO4, and surfactant species were crucial factors determining the formation and morphology of Cu2(OH)PO4. Cu2(OH)PO4 synthesized at different [PO43-](n(Cu)/n(P)=2)...
National Science and Technology Ministry(ID 2012BAK30B03);Fundamental Research Funds for the CentralUniversities(2232013A3-05,CUSF-DH-D-2014036)羟基磷酸铜是一种低表面积、无微孔和中空结构的催化新材料[1],在醇类氧化[2]、苯酚羟化[3]、苯乙烯环氧化[4]、环己烷氧