节点文献
食品中亚硝酸盐含量测定新方法
A New Determination Method of Nitrite in Foods
【摘要】 在酸性条件下,NO2-可以将I-氧化成I2,I2与淀粉反应后生成蓝色络合物,此络合物在595nm处有最大吸收.食品中NO-2的浓度在2.0×10-47.0×10-6g.m L-1范围内与吸光度之间呈良好的线性关系,其标准曲线的回归方程为A=-0.01841+0.10196c,r=0.9995.所得方法的相对标准偏差为0.7%,检出限为5.0×10-8g.m L-1.该方法精密度和准确度高、操作简单、环境污染小.
【Abstract】 Nitrite( NO2-) can oxidize potassium iodide( KI) reagent into iodine( I2) under acidic condition,and I2 can react with starch into iodine-starch blue color complex. The maximum absorption wavelength of this complex is 595 nm. Density of Nitrite in the food is within the range of 2. 0 × 10-4to 7. 0 × 10-6. g. m L-1has liner relation with absorbance. The regression equation of standard curve is: A =-0. 01841 + 0. 10196 c,r = 0. 9995. Using these methods,the detection limit of nitrite is 5. 0 × 10-8g. m L-1and the relative standard deviation is 0. 7 %.Therefore,this new method is simple,rapid,sensitive and accuracy,and has enormous application value in food safety determination.
- 【文献出处】 洛阳师范学院学报 ,Journal of Luoyang Normal University , 编辑部邮箱 ,2016年02期
- 【分类号】TS207.3;O657.3
- 【被引频次】1
- 【下载频次】270