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共沉淀法制备锰锌铁氧体及其磁性能研究
Studies on the Magnetic Properties of Manganese Zinc Ferrite Synthesized by Co-precipitation
【摘要】 采用化学共沉淀法,在80℃水浴以及900℃氩气氛围中煅烧3 h获得锰锌铁氧体.当煅烧时间延长至6 h,锰锌铁氧体因缺氧而产生氧化亚铁.铁氧体的磁性能随Al3+的掺杂量以及锰锌比例而变化,当Al3+的掺杂量为0.1,锰锌物质的量比为0.65∶0.25时,样品的Ms=59.8 Am2·kg-1,Hc=0.32 k A·m-1,Mr=0.13 Am2·kg-1,具有较好的软磁性能.
【Abstract】 Manganese zinc ferrite powder was synthesized by co-precipitaion. The pure ferrite samples were obtained in 80 ℃ water-bath,and then calcined at 900 ℃ for 3 hours under Ar. Ferrous oxide would appear if the calcination time prolonged to 6 hours. The magnetic properties of samples were various with Al3 +content and Mn / Zn ratios. Among all the samples we prepared,Mn0. 65Zn0. 25Al0. 1Fe2O4 displayed good magnetic properties,that was Ms= 59. 8 Am2·kg-1,Hc=0. 32 k A·m-1,Mr= 0. 13 Am2·kg-1.
【关键词】 锰锌铁氧体;
共沉淀;
磁性能;
Al3+掺杂;
【Key words】 manganese zinc ferrite; co-precipitation; magnetic property; aluminum substitution;
【Key words】 manganese zinc ferrite; co-precipitation; magnetic property; aluminum substitution;
【基金】 国家自然科学基金资助项目(61574037);福建省科技厅青年创新项目(2016J05117);福建师范大学2015年省级大学生创新创业训练计划项目资助(201510394050)
- 【文献出处】 福建师范大学学报(自然科学版) ,Journal of Fujian Normal University(Natural Science Edition) , 编辑部邮箱 ,2016年04期
- 【分类号】TM277
- 【被引频次】2
- 【下载频次】271