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常压化学气相沉积法制备SnO2微纳米材料及其催化发光性质研究
Synthesis of SnO2 micro/nano materials by atmospheric pressure chemical vapor deposition and its cataluminescence properties
【摘要】 本文利用一种简单的常压化学气相沉积法在氧化石墨烯基底上制备SnO2材料。通过改变沉积参数(氯化亚锡溶液浓度和沉积时间)得到了多种形貌的SnO2微纳米材料。利用SEM,EDS和XPS对其形貌,成分及元素价态进行表征,并对SnO2材料的催化发光性能进行测试。结果表明,以该材料建立的催化发光气体传感器分别对进样2μL的甲醇,乙醇,异丙醇和丙酮展示了较高的灵敏度,快的响应速度及好的重现性。
【Abstract】 In this paper,a simple atmospheric pressure chemical vapor deposition(APCVD) method was used to synthesize SnO2 materials on graphene oxide substrate. Several morphologies of SnO2 micro/nano materials were obtained by altering the deposition parameters(the concentration of SnCl2 and deposition time),which were characterized by SEM,EDS and XPS. The cataluminescence(CTL) properties of SnO2 materials were explored and the results revealed that the sensor based on SnO2 materials showed relatively high sensitivity,fast responses and good reproducibility to injection 2 μL of methanol,ethanol,isopropanol and acetone.
- 【文献出处】 电子显微学报 ,Journal of Chinese Electron Microscopy Society , 编辑部邮箱 ,2016年06期
- 【分类号】TQ134.32;O643.36
- 【被引频次】4
- 【下载频次】307