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甲醇溶剂下枣庄煤的微波萃取产物分析

Analysis of Products from Methanol- Microwave Extraction of Zaozhuang Coal

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【作者】 鞠彩霞李凤刚宫亚青宗志敏张洪魏贤勇

【Author】 JU Cai-xia;LI Feng-gang;GONG Ya-qing;ZONG Zhi-min;ZHANG Hong;WEI Xian-yong;School of Chemical Engineering and Technology,China University of Mining and Technology;Scool of Chemical Engineering and Material Science,Zaozhuang University;

【机构】 中国矿业大学化学工程学院枣庄学院化学化工与材料科学学院

【摘要】 本研究为分析枣庄煤中的有机成分,采用的是甲醇溶剂对枣庄煤进行了微波萃取,并利用GC/MS对萃取物的组成进行了分析.结果表明枣庄煤甲醇萃取物中GC/MS可检测到化合物70种,其中芳香烃占多数,其次是脂肪烃,含杂化合物占少数,含部分其他物质.这可推测枣庄煤样中可能含有的烃类物质为芳香烃、脂肪烃,含氧化合物有酮、吡啶和酸类,还可能有胺类和芳香硝基化合物.

【Abstract】 For further analysis of organic components in the zaozhaung coa,this paper introduced that methanol solvent is used to extract by Microwave extraction of zaozhuang coal in Zaozhuang,and the composition of the extracts were analyzed by GC /MS. The results show that 70 new compounds could be detected from Zaozhuang coal by GC / MS,of which aromatic hydrocarbons are the majority,followed by aliphatic hydrocarbons,hetero compound minority,and some other compounds are part of.The zaozhaung coal was possibly presumed includes the hydrocarbon compounds: the aromatic hydrocarbon,the aliphatic hydrocarbon,and the oxygen- compounds: ketone,pyridine and acids but also possibly has the amines and the fragrant nitro compound.

【关键词】 枣庄煤甲醇微波萃取GC/MS
【Key words】 zaozhuangcoalmethanolmicrowave extractionGC/MS
【基金】 国家973计划项目(项目编号:2011CB201302);国家自然科学基金重点项目(项目编号:20936007);国家自然科学基金面上项目(项目编号:50974121和51074153);国家自然科学基金委员会创新研究群体科学基金(项目编号:50921002)
  • 【文献出处】 枣庄学院学报 ,Journal of Zaozhuang University , 编辑部邮箱 ,2015年05期
  • 【分类号】O657.63;TQ533
  • 【被引频次】2
  • 【下载频次】127
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