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柑橘精油提取工艺的对比研究
Comparative Study on the Extraction Process of Citrus Essential Oil
【摘要】 采用水提法和加盐水蒸气蒸馏法从柑橘果皮中提取精油。通过单因素试验确定了水蒸气蒸馏法最佳提取条件:提取时间2.0 h、料液比1∶16(g/m L),提取率最高达1.969%。加盐水蒸汽蒸馏法在单因素试验的基础上,通过正交试验法对柑橘果皮中精油的提取进行了研究,结果表明:加盐后最佳工艺条件为Na Cl含量0.3 g,提取时间2.5 h,料液比1∶16(g/m L),提取率最高达3.838%。通过如上对比,建议工业上采用加盐水蒸气蒸馏法从柑橘果皮中提取精油。
【Abstract】 Essential oils were extracted by water distillation and salt- adding steam distillation method respectively in the paper. The single factor experiment showed that,by water distillation,the optimal extraction conditions of essential oil of citrus peel were extraction time of 2. 0 h,solid to liquid ratio 1∶ 16( g / ml),with the most extraction yield 1. 969%. Based on the above experiment,the extraction process was optimized by orthogonal experiments and salt- adding steam distillation method. Experimental results showed that the optimal extraction conditions of citrus essential oil were as follows: the content of Na Cl 0. 3 g,extraction time of 2. 5 h,and solid to liquid ratio 1∶ 16( g / ml)with the most extraction yield 3. 838%. Contrast to the above,salt- adding steam distillation method shall be recommended for extract essential oils from citrus peel applied in industry.
【Key words】 citrus essential oils; extraction; water distillation; salt-adding steam distillation;
- 【文献出处】 中国粮油学报 ,Journal of the Chinese Cereals and Oils Association , 编辑部邮箱 ,2015年12期
- 【分类号】TQ654.2
- 【被引频次】15
- 【下载频次】1863