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室温等离子体还原制备金和钯纳米颗粒的研究(英文)

A simple plasma reduction for synthesis of Au and Pd nanoparticles at room temperature

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【作者】 王召朱煜

【Author】 Zhao Wang;Yu Zhu;State Key Laboratory of Chemical Engineering, School of Chemical Engineering, Tianjin University;

【机构】 State Key Laboratory of Chemical Engineering, School of Chemical Engineering, Tianjin University

【摘要】 A simple and fast plasma reduction method is developed for synthesis of Au and Pd metal nanoparticles. The scanning electron microscopy(SEM) analysis indicates a formation of aggregates of Au and Pd nanoparticles with branched structure. The transmission electron microscopy(TEM) image shows that the inclusive nanoparticles are all about 5 nm in size. Compared to conventional hydrogen reduction method, plasma method inhibits the agglomeration of metal particles. The room temperature operation is very helpful to limit the nanoparticle size. Most interestingly, plasma reduction produces more flattened metal particles. This plasma reduction does not require the use of any hazardous reducing chemicals, showing the great potential for the fabrication of noble metal nanoparticles.

【Abstract】 A simple and fast plasma reduction method is developed for synthesis of Au and Pd metal nanoparticles. The scanning electron microscopy(SEM) analysis indicates a formation of aggregates of Au and Pd nanoparticles with branched structure. The transmission electron microscopy(TEM) image shows that the inclusive nanoparticles are all about 5 nm in size. Compared to conventional hydrogen reduction method, plasma method inhibits the agglomeration of metal particles. The room temperature operation is very helpful to limit the nanoparticle size. Most interestingly, plasma reduction produces more flattened metal particles. This plasma reduction does not require the use of any hazardous reducing chemicals, showing the great potential for the fabrication of noble metal nanoparticles.

【基金】 Supported by the National Natural Science Foundation of China(21206109);the Tianjin Municipal Natural Science Foundation(12JCQNJC04500)
  • 【文献出处】 Chinese Journal of Chemical Engineering ,中国化学工程学报(英文版) , 编辑部邮箱 ,2015年06期
  • 【分类号】O614.123;O614.823;TB383.1
  • 【被引频次】7
  • 【下载频次】86
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