节点文献
N-烷基乙二胺的制备及表征
Preparation and characterization of AEDA
【摘要】 以乙二胺和卤代烷为原料在碱性条件下发生双分子亲核取代反应,合成N-烷基乙二胺,合成产率89.05%。用元素分析、红外光谱和核磁共振波谱对合成的AEDA分子的组成和结构等进行了检测和分析,与预期合成产物AEDA结构吻合。
【Abstract】 With ethylenediamine and halogenated as raw material under alkaline conditions occur double molecular nucleophilic substitution reaction,synthesis of AEDA, synthesis yield was 89.05%. Using elemental analysis, infrared spectrum and nuclear magnetic resonance( NMR) pop on synthesis of AEDA molecular composition and structure of the detection and analysis, in accordance with the expected AEDA synthetic product structure.
【关键词】 亲核取代;
合成产率;
核磁共振波谱分析;
【Key words】 nucleophilic; synthetic yield; nuclear magnetic resonance(NMR) spectral analysis;
【Key words】 nucleophilic; synthetic yield; nuclear magnetic resonance(NMR) spectral analysis;
- 【文献出处】 应用化工 ,Applied Chemical Industry , 编辑部邮箱 ,2015年S1期
- 【分类号】TQ226.31
- 【下载频次】41